Niculescu Mircea and Racu Andrei and Linul Petrica A. and Tăranu Bogdan and Pascariu Mihai-Cosmin: TEM, EDX and raman study of nickel oxide micro- and nanophases obtained by thermal decomposition of an organometallic precursor.
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Abstract
Nickel(II) polyoxalate was thermally decomposed to nickel oxide in both oxidative and inert atmospheres and the products were investigated using TEM-EDX and Raman spectroscopy. The resulting micro- and nanoparticles were compared regarding their size, morphology and composition. In dynamic aerobic conditions, the product obtained at 1000 °C shows better crystallinity and presents more well defined shapes than the one obtained at 400 °C. The 1000 °C product obtained in argon is a mixture of NiO and metallic Ni.
| Item Type: | Conference or Workshop Item |
|---|---|
| Journal or Publication Title: | Proceedings of the International Symposium on Analytical and Environmental Problems |
| Date: | 2016 |
| Volume: | 22 |
| ISBN: | 978-963-306-507-5 |
| Page Range: | pp. 255-258 |
| Event Title: | International Symposium on Analytical and Environmental Problems (22.) (2016) (Szeged) |
| Related URLs: | http://acta.bibl.u-szeged.hu/55893/ |
| Uncontrolled Keywords: | Kémia |
| Additional Information: | Bibliogr.: 258. p. ; ill. ; összefoglalás angol nyelven |
| Date Deposited: | 2018. Dec. 12. 14:09 |
| Last Modified: | 2022. Aug. 08. 15:48 |
| URI: | http://acta.bibl.u-szeged.hu/id/eprint/56089 |
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