Synthesis and characterization of Co(II) carboxylates resulted in the Co(N03)2 - 1,3-propanediol redox reaction

Dippong Thomas and Pauliuc Ivan and Pacala Adina: Synthesis and characterization of Co(II) carboxylates resulted in the Co(N03)2 - 1,3-propanediol redox reaction.

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Abstract

This paper presents the study of the redox reaction Co (N0 3)2 - 1, 3 propanediol (HOCH2CHCH2OH) and the characterization of its product by means of thermal analysis, FTIR spectrometry and acidic - basic titrations. The study of the acidic - basic properties of the redox reaction product, correlated with the thermal analysis and FTIR spectrometry, highlights the formation of cobalt malonate (1.3 propane dicarboxilic acid). This product that thermally decomposes at 300°C was used as precursor for cobalt oxides. As evidenced by XRD analysis of the annealing products at 400°C and 700°C, nanocrystallites Co3C>4 is obtained at both temperatures.

Item Type: Conference or Workshop Item
Journal or Publication Title: Proceedings of the International Symposium on Analytical and Environmental Problems
Date: 2012
Volume: 17
ISBN: 978-963-315-066-5
Page Range: pp. 76-80
Language: English
Publisher: SZAB
Place of Publication: Szeged
Event Title: International Symposium on Analytical and Environmental Problems (17.) (2011) (Szeged)
Event Type: Conference
Event Location: Szeged
Event Dates: 2011. szeptember 19.
Related URLs: http://acta.bibl.u-szeged.hu/76381/
Uncontrolled Keywords: Analitikai kémia
Additional Information: Bibliogr.: 80. p. ; ill. ; összefoglalás angol nyelven
Subjects: 01. Natural sciences
01. Natural sciences > 01.04. Chemical sciences
Date Deposited: 2022. Aug. 09. 11:00
Last Modified: 2022. Aug. 22. 10:23
URI: http://acta.bibl.u-szeged.hu/id/eprint/76394

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