HPLC-ESI-TOF-MS chemical characterization of comfrey root extract obtained by subcritical water extraction

Nastić Nataša and Segura-Carretero Antonio and Borrás-Linares Isabel and Lozano-Sánchez Jesús and Pastor Kristian A. and Švarc-Gajić Jaroslava: HPLC-ESI-TOF-MS chemical characterization of comfrey root extract obtained by subcritical water extraction.

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Abstract

In this work, a study on phytochemical profiles of comfrey (Symphytum officinale L.) root extract obtained by subcritical water extraction (SWE) has been carried out. Chemical composition was assessed by high-performance liquid chromatography coupled with electrospray time-of-flight mass spectrometry (HPLC-ESI-TOF-MS) identifying 22 compounds including organic acids, phenolic acids, flavonoids and fatty acids. Great number of phenolic acids and flavonoids were found in the extract obtained by SWE, with citric acid, caffeic acid and derivative, salvianolic acid B, hydroxybenzoic acid, syringetin-3-O-glucoside and quercetin 3-O-malonylglucoside as the most abundant compounds. Moreover, quercitin-3- malonylglucoside isomers, hydroxybenzoic acid glucoside, cirismaritin isomers, p-coumaric acid, hydroxycoumarin and methylcoumarin, among others, were identified for the first time in S. officinale root. Overall, the results indicate the potential of SWE for the production of highquality plant extracts from S. officinale root.

Item Type: Conference or Workshop Item
Journal or Publication Title: Proceedings of the International Symposium on Analytical and Environmental Problems
Date: 2022
Volume: 28
ISBN: 978-963-306-904-2
Page Range: pp. 265-268
Language: English
Place of Publication: Szeged
Event Title: 28th International Symposium on Analytical and Environmental Problems
Event Type: Conference
Event Location: Szeged
Event Dates: 2022. november 14-15.
Related URLs: https://acta.bibl.u-szeged.hu/78308/
Uncontrolled Keywords: Analitikai kémia, Fotokémia
Additional Information: Bibliogr.: 268. p. ; ill. ; összefoglalás angol nyelven
Subjects: 01. Natural sciences
01. Natural sciences > 01.04. Chemical sciences
Date Deposited: 2023. Mar. 23. 09:44
Last Modified: 2023. Mar. 23. 09:44
URI: http://acta.bibl.u-szeged.hu/id/eprint/78531

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