TY - CONF M2 - Szeged SP - 362 N1 - Bibliogr.: 365. p. ; ill. ; összefoglalás angol nyelven UR - http://acta.bibl.u-szeged.hu/76464/ SN - 978-963-315-066-5 CY - Szeged AV - public ID - acta76464 TI - Synthesis of ultrafine gahnite (ZnAI20 4) nanocrystals by coprecipitation method EP - 365 VL - 17 Y1 - 2012/// T2 - International Symposium on Analytical and Environmental Problems (17.) (2011) (Szeged) N2 - Nanocrystalline zinc aluminate ZnAl20 4 has been obtained by coprecipitation method at two different temperatures (800°C and 900°C). The precursors used in coprecipitation synthesis of ZnAECE were zinc nitrate hexahydrate and aluminum nitrate nonahydrate. As a basic source sodium hydroxide was used. The obtained samples were analyzed by X-ray diffraction (XRD) and by energy dispersive spectroscopy (EDAX). Optical properties of nanocrystalline zinc aluminate were also determined by UV/VIS/NIR spectroscopy. The band gap for sample obtained at 800°C was 3,88 eV while for sample obtained at 900°C was 3,97 eV. KW - Elektrokémia A1 - Miron Iasmina A1 - Ursu Daniel A1 - Grozescu Ioan PB - SZAB ER -